HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178510730, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 135976158 | HCID 135976158 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178510730 | HCID 178510730 | 57% |
Reaction Steps
Prepared as in Example 1 from 2-benzoyl-5-chloro-benzo[b]-thiophen-3-ol, phosphorus(V) chloride and concentrated ammonia with a yield of 57% of theory. M.p. 172°-173° C. (ethyl acetate)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288437 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-e0b06f1af3904ad980b99d6a0cf52e2f |
| Source note | uspto-grants-1981_09 |