2-Morpholinoethylamine → HCID 178516508, compound

HRID 1577550Notes

Reaction equation

HRID 1577550 reaction equation
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[C:10]=1[OH:18])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[N:19]1([CH2:25][CH2:26][NH2:27])[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1>>[N:19]1([CH2:25][CH2:26][NH:27]/[C:1](/[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[C:9]2\[C:10](=[O:18])[C:11]3[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=3[S:13]\2)[CH2:24][CH2:23][O:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 4082852-MorpholinoethylamineHCID 4712192Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl-

Product 1

HCID 178516508HCID 178516508, compoundYield 62%

Procedure

Prepared as in Example 35 from 2-benzoyl-benzo[b]thiophen-3-ol and 2-(4-morpholinyl)-ethylamine instead of ammonium acetate with a yield of 62% of theory.

Sources & evidence

ORD record
ord-b726b9b2c9e0496f86742fc47ca37231
Source dataset
uspto-grants-1981_09
Patent number
US04288437

Reaction notes

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