Pyrrolidine → HCID 20570792, compound

HRID 1577560Notes

Reaction equation

HRID 1577560 reaction equation
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[C:10]=1[OH:18])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH:19]1[CH2:23][CH2:22][CH2:21][CH2:20]1>C(O)(=O)C>[N:19]1(/[C:1](/[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[C:9]2\[C:10](=[O:18])[C:11]3[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=3[S:13]\2)[CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

4

Reactant 2

HCID 31268PyrrolidineHCID 4712192Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl-

Product 1

HCID 20570792HCID 20570792, compoundYield 5%

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Prepared as in Example 31 from 2-benzoyl-benzo[b]thiophen-3-ol and pyrrolidine in glacial acetic acid with a yield of 5% of theory. Egg-yellow crystals, m.p. 157° C. (ethyl acetate/petroleum ether 1:3).

Sources & evidence

ORD record
ord-1bdda8bb710a4bed997c6e1305dd6420
Source dataset
uspto-grants-1981_09
Patent number
US04288437

Reaction notes

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