Ammonium Acetate → HCID 178487339, compound

HRID 1577564Notes

Reaction equation

HRID 1577564 reaction equation
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[C:15]([O:18][CH3:19])[CH:16]=[CH:17][C:11]=2[C:10]=1[OH:20])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C([O-])(=O)C.[NH4+:25]>>[NH2:25]/[C:1](/[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)=[C:9]1\[C:10](=[O:20])[C:11]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:12]=2[S:13]\1

Participants

3

Reactant 2

HCID 517165Ammonium AcetateHCID 136047785HCID 136047785, compound

Product 1

HCID 178487339HCID 178487339, compoundYield 64%

Procedure

Prepared as in Example 31 from 2-benzoyl-6-methoxy-benzo[b]thiophen-3-ol and ammonium acetate with a yield of 64% of theory.

Sources & evidence

ORD record
ord-49ad7e0b855a4381bf4a6ec1c0e4fdc0
Source dataset
uspto-grants-1981_09
Patent number
US04288437

Reaction notes

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