HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromo(phenyl)acetic acid → HCID 12922546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromo(phenyl)acetic acid | HCID 97919 | — |
| Reactant | 2-Piperidinethione | HCID 3030637 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 12922546 | HCID 12922546 | — |
Reaction Steps
An acetone solution of 3.51 g. (0.03 mole) δ-thiovalerolactam and 6.75 g. (0.03 mole) α-bromophenylacetic acid was heated until the solid started to form. After the solution was cooled, the solid was collected which weighed 6.5 g. Recrystallization could be done with acetonitrile. The purified material had a melting point of 188°-192° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04289697 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-6f87397d50824a4fb21c34005438cad7 |
| Source note | uspto-grants-1981_09 |