L-Ascorbic Acid → 16690-40-7

HRID 1577778Notes

Reaction equation

[O:1]=[C:2]1[O:8][C@H:7]([C@H:9]([CH2:11][OH:12])[OH:10])[C:5]([OH:6])=[C:3]1[OH:4].[CH2:13](O)[C@@H:14](O)[C@H:15]1[O:20][C:18](=O)[C:17](O)=[C:16]1O>>[C:18]([O:12][CH2:11][C@H:9]([OH:10])[C@H:7]1[O:8][C:2](=[O:1])[C:3]([OH:4])=[C:5]1[OH:6])(=[O:20])[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:2][CH2:3][CH2:5][CH2:7][CH2:9][CH3:11]

Participants

Reactant 2

HCID 54670067L-Ascorbic Acid

HCID 54675810Erythorbic Acid

Product 1

HCID 5470262816690-40-7Yield 70%

Procedure

Repetition of the preparation substituting ascorbic acid for the erythorbic acid resulted in the isolation of 26.35 g of a white waxy solid assaying 95.1% ascorbic acid 6-laurate (0.070 mole, 70% yield).

Sources & evidence

ORD record: ord-3453a1d7037749e4a167c031a621541d
Source dataset: uspto-grants-1981_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04289702

Reaction notes

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