HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromophenyl Isothiocyanate → N-(3-bromophenyl)-2-decyltetrahydro-2H-1,3-thiazine3-carbothioamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromophenyl Isothiocyanate | HCID 16481 | — |
| Reactant | 2-decyltetrahydro-2H-1,3-thiazine | HCID 20569623 | — |
| Product | N-(3-bromophenyl)-2-decyltetrahydro-2H-1,3-thiazine3-carbothioamide | HCID 12783515 | — |
Reaction Steps
The procedure of Example 25 was repeated, except that the reactants consisted of 0.9 g. of 2-decyltetrahydro-2H-1,3-thiazine and 0.7 g. of 3-bromophenyl isothiocyanate. The product was recrystallized from ethanol to give N-(3-bromophenyl)-2-decyltetrahydro-2H-1,3-thiazine3-carbothioamide, m.p. 73°-4°. The following elemental microanalysis was obtained:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04289766 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-31baf5a016914eddb43065a33786e0d9 |
| Source note | uspto-grants-1981_09 |