Ethyl Bromide → HCID 12951746, compound

HRID 1577899Notes

Reaction equation

HRID 1577899 reaction equation
[CH2:1]([N:3]([CH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:2].[CH2:19]([Br:21])[CH3:20]>>[Br-:21].[CH2:1]([N+:3]([CH2:10][CH2:11][CH2:12][C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1)([CH2:19][CH3:20])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH3:2]

Participants

3

Reactant 2

HCID 6332Ethyl BromideHCID 20494480HCID 20494480, compound

Product 1

HCID 12951746HCID 12951746, compound

Procedure

5.21 Grams of N-ethyl-N-n-hexyl-3-phenylpropylamine was placed in a 200 ml. round bottom flask. 100 Milliliters of ethyl bromide was added. The mixture was refluxed five days. Excess ethyl bromide was removed by evaporation in vacuo leaving as an oil N,N-diethyl-N-n-hexyl-3-phenylpropylammonium bromide.

Workup

  1. temperatureThe mixture was refluxed five days
  2. customExcess ethyl bromide was removed by evaporation in vacuo

Sources & evidence

ORD record
ord-b54a5b677b734e438dc88b23bc811023
Source dataset
uspto-grants-1981_09
Patent number
US04289787

Reaction notes

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