Tetrahydrofuran → HCID 70547117, compound

Participants

Reaction Steps

The procedure is carried out as described in Example 1, with the use however in this case of 5 g of potassium tert-butylate, 240 g (1.59 mols) of cyclohexyl-methylidene-allylamine and 250 ml of tetrahydrofuran. After a reaction time of 1 hour at 30° C., there is obtained 199 g (1.32 mols) of propylidene(cyclohexylidene-methylamine), corresponding to a yield of 83% of theory; b.p. 51°-53° C./0.3 Torr; nD20 =1.5072.

Provenance & Evidence