HCID 20436125, compound → HCID 53884118, compound

Participants

Reaction Steps

The procedure is carried out as described in Example 1 with the use however in this case of 10 g of potassium tert-butylate, 800 g (4.79 mols) of (2-ethylhexylidene)-allylamine and 600 ml of tetrahydrofuran. After a reaction time of 2 hours at 35° C., there is obtained 682 g (4.08 mols) of N-propylidene-(2-ethylhexen-1-yl-amine), corresponding to a yield of 85.2% of theory (isomeric mixture in the weight ratio of 55:45); b.p. 53°-56° C./1 Torr; nD20 =1.4698.

Provenance & Evidence