Isopropanol → HCID 53934923, compound

HRID 1578031Notes

Reaction equation

[CH3:1][C:2]([CH3:19])([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH:14]([CH:16]([CH3:18])[CH3:17])[NH2:15])[C:3]([OH:5])=[O:4].[CH:20](O)([CH3:22])[CH3:21]>>[CH:20]([O:4][C:3](=[O:5])[C:2]([CH3:19])([CH3:1])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH:14]([CH:16]([CH3:17])[CH3:18])[NH2:15])([CH3:22])[CH3:21]

Participants

Reactant 2

HCID 3776Isopropanol

HCID 20518084HCID 20518084, compound

Product 1

HCID 53934923HCID 53934923, compoundYield 76%

Procedure

The procedure described in Example (1b) is repeated, using 50 g (0.185 mole) of 2,2-dimethyl-11-isopropyl-11-aminoundecanoic acid and 100 ml of isopropanol. Distillation yields 44 g (0.141 mole) of 2,2-dimethyl-11-isopropyl-11-aminoundecanoic acid isopropyl ester, corresponding to a yield of 76% of theory;

Workup

distillationDistillation

Sources & evidence

ORD record: ord-6e2ba06db3104802b38a5e9400aec877
Source dataset: uspto-grants-1981_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04290964

Reaction notes

Loading…