Ethylene → HCID 18705481, compound
Reaction equation
[CH2:1]=[CH:2][CH3:3].[CH3:4][CH2:5][CH2:6][CH2:7][CH:8]=[CH2:9].[CH2:10]=[CH2:11].[H][H]>>[CH2:1]=[CH:2][CH3:3].[CH3:9][CH2:8][CH2:7][CH2:6][CH:5]=[CH2:4].[CH2:10]=[CH2:11]Participants
5
Conditions
- Temperature
- 60 °C
Procedure
The temperature was then raised to 60° C., and propylene, hexene-1, and ethylene were fed at rates of 3.5 kg/hour, 1.7 kg/hour, and 0.13 kg/hour, respectively, for 5 hours. During this step, hydrogen was also supplied to maintain the hydrogen concentration in the gaseous region at 5.5 percent. Thus, the propylene/hexene-1/ethylene terpolymeric random copolymer block was prepared.
Workup
- temperatureto maintain
- concentrationthe hydrogen concentration in the gaseous region at 5.5 percent
Sources & evidence
- ORD record
- ord-ee9085810643401b8f076275523046b9
- Source dataset
- uspto-grants-1981_09
- Patent number
- US04291140
Reaction notes
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