Methyl Acrylate → Methyl 5-oxohexanoate

HRID 1578170Notes

Reaction equation

HRID 1578170 reaction equation
[C:1]([O:5][CH3:6])(=[O:4])[CH:2]=[CH2:3].[O:7]=[C:8]([CH3:15])[CH2:9]CCC(O)=O>>[CH3:6][O:5][C:1]([CH2:2][CH2:3][CH2:9][C:8](=[O:7])[CH3:15])=[O:4]

Participants

3

Reactant 2

HCID 7294Methyl Acrylate2×HCID 184074-Acetylbutyric acid

Product 1

HCID 84129Methyl 5-oxohexanoate

Procedure

Subsequently, the tubes are cooled rapidly, following which the contents of the tubes is analyzed gaschromatographically, and the conversion of the methyl acrylate, as well as the efficiency in the methyl ester of 4-oxopentane-1-carboxylic acid product, referred to the converted methyl acrylate, is determined.

Workup

  1. temperatureSubsequently, the tubes are cooled rapidly

Sources & evidence

ORD record
ord-3a35994cc51a4fe18894e458385f7340
Source dataset
uspto-grants-1981_09
Patent number
US04291170

Reaction notes

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