HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 1-Chloro-4-nitro-2-propoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 2-Chloro-5-nitrophenol | HCID 69264 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 1-Chloro-4-nitro-2-propoxybenzene | HCID 12881603 | — |
Reaction Steps
A mixture of 3.47 g. of 2-chloro-5-nitrophenol, 3.74 g. of propyl iodide, 3.04 g. of anhydrous potassium carbonate and 20 ml. of acetone was refluxed with stirring for 6 hours to obtain 3.80 g of 4-chloro-3-propoxynitrobenzene having a melting point of 52° to 53° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04292070 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-5ee5c368d31a4c66add490e96a5908aa |
| Source note | uspto-grants-1981_09 |