Propylamine → HCID 21559905, compound

Participants

Reaction Steps

A reaction mixture containing 5.14 g (16.8 mmol) of 6-chloro-9-veratrylpurine, 7.0 ml (84.9 mmol) of propylamine and 60 ml of EtOH was refluxed for 2.5 hrs. Evaporation of the reaction mixture gave a residual solid which was recrystallized from acetone to give the crude product; yield 4.78 g (87.0%) mp 117°-120°. Further recrystallizations of the crude white material from acetone gave the analytical material; mp 122°-125°.

Provenance & Evidence