HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexamethylenediamine → N-phenylstearyl hexamethylene diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexamethylenediamine | HCID 16402 | — |
| Reactant | HCID 53680545 | HCID 53680545 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-phenylstearyl hexamethylene diamine | HCID 86733042 | — |
Reaction Steps
Following the procedure of Example XVI a solution of 15.8 grams (0.04 mole) of phenylstearyl bromide and 37.2 grams (0.32 mole) of hexamethylene diamine in 400 ml of ethanol was refluxed for three hours. After the same recovery procedure 15.2 grams (88.4% crude mass yield) of N-phenylstearyl hexamethylene diamine was obtained having the following analysis:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03936503 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-a40055875796432c81ab38d600664d83 |
| Source note | uspto-grants-1976_02 |