N,O-Dimethylhydroxylamine →

Participants

Reaction Steps

To a solution of 12.9 grams (0.064 mole) of IV in 250 milliliters of ether was added a solution of 4.9 grams (0.08 mole) of O,N-dimethylhydroxylamine in 350 milliliters of methanol. The resulting mixture was concentrated to dryness, washed with water and recrystallized from acetone/hexane (5:1) to give 11.8 grams (71% yield) of V as a white crystalline solid, melting point: 125°-126°. Its identity was confirmed by elemental analysis.

Provenance & Evidence