HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53647982, compound → HCID 54336752, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53647982 | HCID 53647982 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54336752 | HCID 54336752 | — |
Reaction Steps
Yield: 115 grams of 3-(1',2'-dichlorovinyloxy)-nitrobenzene 1 mole of the nitro-product was dissolved in 1liter of ethanol and was reduced by means of hydrogen in an autoclave at 60°C, after 5 grams of a Raney-nickel catalyst (R/50) had been added. The catalyst was then filtered off with suction, the ethanol was distilled off, and the residue was distilled in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03937726 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-71117df808e445c48dc3d4b1dba7cba0 |
| Source note | uspto-grants-1976_02 |