Benzoyl Peroxide → 3-Vinylpyridine styrene

HRID 1578572Notes

Reaction equation

HRID 1578572 reaction equation
[CH:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1)=[CH2:2].[CH2:9]=[CH:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>O>[CH:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1)=[CH2:2].[CH2:9]=[CH:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

5

Reactant 3

HCID 7187Benzoyl PeroxideHCID 7501StyreneHCID 142723-Vinylpyridine

Product 1

HCID 704252523-Vinylpyridine styrene

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
60 °C

Procedure

Into a glass tube were placed 10.514 g. freshly distilled 3-vinylpyridine, 10.415 g. freshly distilled styrene and 0.100 g. benzoyl-peroxide. The mixture was maintained at 60°C in an oil bath for 24 hr. The resulting polymer solution was poured into 10 times the volume of rapidly stirred water, filtered and dried to give a 3-vinylpyridine-styrene copolymer.

Workup

  1. customInto a glass tube were placed
  2. filtrationfiltered
  3. customdried

Sources & evidence

ORD record
ord-b567b40b4318437d8d4ba17392b3e91c
Source dataset
uspto-grants-1976_02
Patent number
US03937764

Reaction notes

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