HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → 5-Methoxy-2-(1H-pyrrol-1-yl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 2803813 | HCID 2803813 | — |
| Solvent | Water | HCID 962 | — |
| Product | 5-Methoxy-2-(1H-pyrrol-1-yl)aniline | HCID 2764415 | — |
Reaction Steps
A stirred solution of 33.5 g (0.154 mole) of 1-(4-methoxy-2-nitrophenyl)pyrrole in 684 ml. of tetrahydrofuran and 340 ml. of water is treated according to the manipulative procedure described in Example 13(b) to give 1-(2-amino-4-methoxyphenyl)pyrrole, m.p. 42°-43° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03939159 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-39bf1a8469694c76aabc614a106c8ceb |
| Source note | uspto-grants-1976_02 |