Tetrahydrofuran → HCID 10775663, compound

HRID 1578701Notes

Reaction equation

HRID 1578701 reaction equation
[Cl:1][C:2]1[C:7]([Cl:8])=[CH:6][C:5]([N:9]2[CH:13]=[CH:12][CH:11]=[CH:10]2)=[C:4]([N+:14]([O-])=O)[CH:3]=1.O1CCCC1>O>[NH2:14][C:4]1[CH:3]=[C:2]([Cl:1])[C:7]([Cl:8])=[CH:6][C:5]=1[N:9]1[CH:13]=[CH:12][CH:11]=[CH:10]1

Participants

4

Reactant 2

HCID 8028TetrahydrofuranHCID 10491350HCID 10491350, compound

Product 1

HCID 10775663HCID 10775663, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A stirred solution of 42.4 g (0.165 mole) of 1-(4,5-dichloro-2-nitrophenyl)pyrrole in 730 ml. of tetrahydrofuran and 365 ml. of water is treated according to the manipulative procedure described above in Example 13(b) to give 1-(2-amino-4,5-dichlorophenyl)pyrrole, m.p. 57°-58° C.

Sources & evidence

ORD record
ord-7de54c87901942a88632590dd9ce8f67
Source dataset
uspto-grants-1976_02
Patent number
US03939159

Reaction notes

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