HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 24192289, compound → HCID 135783944, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 24192289 | HCID 24192289 | — |
| Reactant | 4-Chloro-7-nitro-2,5-bis(trifluoromethyl)benzimidazole | HCID 135554935 | — |
| Product | HCID 135783944 | HCID 135783944 | — |
Reaction Steps
4-Chloro-7-nitro-2,5-bis(trifluoromethyl)benzimidazole is reacted with potassium diethyl malonate to obtain 4-(bis(carboethoxy)methyl)-7-nitro-2,5-bis(trifluoromethyl)-benzimidazole; this intermediate is deesterified and decarboxylated to yield 4-methyl-7-nitro-2,5-bis(trifluoromethyl)-benzimidazole, m.w., 313.2. In like procedures, the following are prepared:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03939166 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-ffce85cfb56c49e383455980e26336ef |
| Source note | uspto-grants-1976_02 |