HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → 2-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | 2-[4-[4-(2-Pyridinyl)-1-piperazinyl]butyl]-1H-benz[de]-isoquinoline-1,3-(2H)-dione, hydrochloride | HCID 131710060 | — |
| Product | 2-(5-Bromopentyl)benzo[de]isoquinoline-1,3-dione | HCID 16638791 | — |
Reaction Steps
Following the procedure of part (a) of example 46 but substituting 1,5-dibromopentane for the 1,4-dibromobutane, one obtains 2-(5-bromopentyl)-1H-benz[de]isoquinoline-1,3(2H)-dione; m.p. 113°-115°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03940398 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-f4515deedec74caead3f82680a7d0a0e |
| Source note | uspto-grants-1976_02 |