HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetohydrazide → HCID 178475140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetohydrazide | HCID 14039 | — |
| Reactant | Ethyl 1-methyl-5-nitro-1H-imidazole-2-carboximidate | HCID 21432269 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178475140 | HCID 178475140 | — |
Reaction Steps
In 200 ml. of methanol, 12 g. (0.06 mole) of ethyl 1-methyl-5-nitro-2-imidazolecarboximidate and 4.9 g. (0.066 mole) of acetyl hydrazine are refluxed for 30 hours. The yellow compound is collected, washed with cold methanol and dried to give 12.97 g. of the title compound, melting point 294°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03940411 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-6646db82708743fe97c41ba1da41885f |
| Source note | uspto-grants-1976_02 |