Diethyl Ether → HCID 14976040, compound

A mixture containing 13.9 ml. of 3-bromo-1-propanol, 7.6 ml. of methane sulfonyl chloride and 100 ml. ether was formed. The mixture was mixed together and 14 ml. of triethylamine was added over a period of 45 minutes at 5°-10°C. and then stirred at 5°-10°C. for 1 hour. The mixture was allowed to come to room temperature and was stirred for an additional 15 minutes. To the mixture was added 100 ml. of water and the ether solution dried over magnesium sulfate and evaporated to yield 14.5 g. of a colorless oil. nD30 1.4749.

1. additionA mixture containing 13.9 ml
2. additionThe mixture was mixed together
3. customto come to room temperature
4. stirringwas stirred for an additional 15 minutes
5. additionTo the mixture was added 100 ml
6. dry with materialof water and the ether solution dried over magnesium sulfate
7. customevaporated
8. customto yield 14.5 g

ORD record

ord-a26ab4fa99164a5bada08760fd14528d

Source dataset

uspto-grants-1976_01

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US03930836