Isoquinoline, 1-chloro- → HCID 21567180, compound

HRID 1579135Notes

Reaction equation

HRID 1579135 reaction equation
CC1N=CC2C(C=1)=C([N+]([O-])=O)C=CC=2.[Cl:15][C:16]1[C:25]2[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH:19]=[CH:18][N:17]=1>>[ClH:15].[Cl:15][C:16]1[C:25]2[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=2)[CH:19]=[CH:18][N:17]=1

Participants

3

Reactant 2

HCID 140539Isoquinoline, 1-chloro-HCID 2749733-Methyl-5-nitroisoquinoline

Product 1

HCID 21567180HCID 21567180, compound

Procedure

was prepared by the procedure of Example II except that the 3-methyl-5-nitro-isoquinoline of that example was replaced by 1-chloro-isoquinoline to yield 1-chloro-isoquinoline hydrochloride melting over the range 78° - 84°C.

Sources & evidence

ORD record
ord-23b3c76854384d9f9658cd458e223066
Source dataset
uspto-grants-1976_01
Patent number
US03930837

Reaction notes

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