Hydrogen iodide → HCID 21567192, compound

HRID 1579136Notes

Reaction equation

HRID 1579136 reaction equation
CC1N=CC2C(C=1)=C([N+]([O-])=O)C=CC=2.[Cl:15][C:16]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[C:22]2[C:17]=1[CH:18]=[CH:19][N:20]=[CH:21]2.Cl.CC1N=CC2C(C=1)=C([N+]([O-])=O)C=CC=2.[IH:44]>>[IH:44].[Cl:15][C:16]1[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[C:22]2[C:17]=1[CH:18]=[CH:19][N:20]=[CH:21]2

Participants

5

Reactant 4

HCID 24841Hydrogen iodideHCID 2749733-Methyl-5-nitroisoquinolineHCID 3180535-CHLORO-8-NITROISOQUINOLINEHCID 21567166HCID 21567166, compound

Product 1

HCID 21567192HCID 21567192, compound

Procedure

was prepared by the procedure of Example 11 hereinabove, except that the 3-methyl-5-nitro-isoquinoline of that example was replaced by 5-chloro-8-nitro-isoquinoline, and the concentrated hydrochloric acid of Example 11 was replaced by concentrated hydriodic acid, to yield 5-chloro-8-nitro-isoquinoline hydro-iodide, melting over the range 161°-5°C.

Sources & evidence

ORD record
ord-6468d0ea0a7c4b14b1923bb49912b862
Source dataset
uspto-grants-1976_01
Patent number
US03930837

Reaction notes

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