Thionyl Chloride → HCID 603802, compound

HRID 1579145Notes

Reaction equation

HRID 1579145 reaction equation
[CH3:1][O:2][C:3]1[C:4]([C:13]([OH:15])=O)=[CH:5][C:6]2[C:11]([CH:12]=1)=[CH:10][CH:9]=[CH:8][CH:7]=2.S(Cl)([Cl:18])=O>C1C=CC=CC=1>[CH3:1][O:2][C:3]1[C:4]([C:13]([Cl:18])=[O:15])=[CH:5][C:6]2[C:11]([CH:12]=1)=[CH:10][CH:9]=[CH:8][CH:7]=2

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 701613-Methoxy-2-naphthoic acid

Product 1

HCID 603802HCID 603802, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

To 4.55 grams of (VII) slurried in 25 milliliters of benzene, 3.57 grams of thionyl chloride was added. The mixture was refluxed for several hours and the solvent was removed to yield a thick yellow resinous product, 3-methoxy-2-naphthoyl chloride (VIII).

Workup

  1. temperatureThe mixture was refluxed for several hours
  2. customthe solvent was removed

Sources & evidence

ORD record
ord-3736a18cb2a843669e3cba59df65f2be
Source dataset
uspto-grants-1976_01
Patent number
US03931103

Reaction notes

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