HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 603802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Methoxy-2-naphthoic acid | HCID 70161 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 603802 | HCID 603802 | — |
Reaction Steps
To 4.55 grams of (VII) slurried in 25 milliliters of benzene, 3.57 grams of thionyl chloride was added. The mixture was refluxed for several hours and the solvent was removed to yield a thick yellow resinous product, 3-methoxy-2-naphthoyl chloride (VIII).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931103 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-3736a18cb2a843669e3cba59df65f2be |
| Source note | uspto-grants-1976_01 |