HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 21567778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 12493646 | HCID 12493646 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 21567778 | HCID 21567778 | — |
Reaction Steps
A solution of 5 g of 6-carbethoxy-2,3-dihydro-1H-pyrrolo [1,2-a]benzimidazole (1A06) in 15 cm3 of ethanol and 25 cm3 of 2,5 N sodium hydroxide are refluxed for 5 min. After cooling the reaction mixture is slightly acidified with diluted acetic acid and the precipitate formed is sucked off and washed with water and ethanol. Yield: 4 g. Melting point: 300°c.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931156 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-cd4defa30a36408e98e33a802389daba |
| Source note | uspto-grants-1976_01 |