Cyclooctanone → HCID 21567553, compound

HRID 1579167Notes

Reaction equation

HRID 1579167 reaction equation
[C:1]([NH:5][NH:6][C:7]([C:12]#[N:13])([CH:9]1[CH2:11][CH2:10]1)[CH3:8])([CH3:4])([CH3:3])[CH3:2].[C:14]1(=O)[CH2:21]CCCCC[CH2:15]1.C1(C(C)=O)CC1>>[C:1]([NH:5][NH:6][C:7]1([C:12]#[N:13])[CH2:8][CH2:21][CH2:14][CH2:15][CH2:10][CH2:11][CH2:9]1)([CH3:2])([CH3:3])[CH3:4]

Participants

4

Reactant 3

HCID 10403CyclooctanoneHCID 13004Cyclopropyl methyl ketoneHCID 23344788HCID 23344788, compound

Product 1

HCID 21567553HCID 21567553, compoundYield 100%

Procedure

1-t-Butylhydrazo-1-cyanocyclooctane was prepared in 100% yield using the same procedure described in Example XIIIB for the preparation of 1-t-butylhydrazo-1-cyano-1-cyclopropylethane, substituting the t-butylhydrazone of cyclooctanone for the t-butylhydrazone of methyl cyclopropyl ketone.

Sources & evidence

ORD record
ord-154d895bc30f47259ae35700411c8bcc
Source dataset
uspto-grants-1976_01
Patent number
US03931143

Reaction notes

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