Cycloheptanone → HCID 21567558, compound

HRID 1579169Notes

Reaction equation

HRID 1579169 reaction equation
[C:1]([NH:5][NH:6][C:7]([C:12]#[N:13])([CH:9]1[CH2:11][CH2:10]1)[CH3:8])([CH3:4])([CH3:3])[CH3:2].[C:14]1(=O)CCCCC[CH2:15]1.C1(C(C)=O)CC1>>[C:1]([NH:5][NH:6][C:7]1([C:12]#[N:13])[CH2:8][CH2:15][CH2:14][CH2:10][CH2:11][CH2:9]1)([CH3:2])([CH3:3])[CH3:4]

Participants

4

Reactant 3

HCID 10400CycloheptanoneHCID 13004Cyclopropyl methyl ketoneHCID 23344788HCID 23344788, compound

Product 1

HCID 21567558HCID 21567558, compoundYield 95%

Procedure

1-t-Butylhydrazo-1-cyanocycloheptane was prepared in 95% yield using the same procedure described in Example XIIIB for the preparation of 1-t-butylhydrazo-1-cyano-1-cyclopropylethane, substituting the t-butylhydrazone of cycloheptanone for the t-butylhydrazone of methyl cyclopropyl ketone.

Sources & evidence

ORD record
ord-ba00a48bc1204923a0dd42e3d9dd21e6
Source dataset
uspto-grants-1976_01
Patent number
US03931143

Reaction notes

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