HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 86732863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 53710559 | HCID 53710559 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 86732863 | HCID 86732863 | — |
Reaction Steps
A solution of the free base of the product of Example 3 in acetic acid is treated with an equivalent quantity of 30% hydrogen peroxide and the solution then heated at 80°-90° for 1 hour and cooled. The solvent is then removed on a rotary evaporator at reduced pressure to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931169 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-13f2a80106d64503b9701e1bce133dfd |
| Source note | uspto-grants-1976_01 |