HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → 5-Methyl-2-furanmethanethiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | 5-Methyl-2-furanmethanethiol | HCID 521873 | — |
| Product | 5-Methyl-2-furanmethanethiol | HCID 521873 | — |
| Product | Methyl 5-methylfurfuryl sulfide | HCID 6428935 | — |
Reaction Steps
2 a. 5-Methylfurfuryl methyl sulfide was prepared by reacting 5-methylfurfuryl-mercaptan with dimethyl sulfate in alkaline solution according to known methods. 5-Methylfurfuryl-mercaptan was obtained from the corresponding alcohol by the method described in Org. Syn. 35, 67 (1955). The product is a colorless liquid boiling at 71°-72°C./11 mm. Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931166 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-8d0768534dcb4491a2f1794c78c260df |
| Source note | uspto-grants-1976_01 |