HRID1579369

反应详情

EQUATION

反应方程式

HRID 1579369 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2'-(2-Pyridylmethyl)-p-anisanilide (9.5 g., 0.03 mole) and 0.3 mole of methyl iodide in 100 ml. of acetone is refluxed with stirring for a period of 64 hr. The reaction mixture filtered and the filter cake washed with acetone provides a 93% yield of 2-[2-(p-methoxybenzamido)benzyl]-1-methylpyridinium iodide, m.p. 184°-186°C. (corr.).

WORKUP

后处理

  1. filtrationThe reaction mixture filtered
  2. washthe filter cake washed with acetone