HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 54294797, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 86732879 | HCID 86732879 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54294797 | HCID 54294797 | — |
Reaction Steps
In a manner similar to that described in Example 1D, treat 6β,7β-dimethanesulfonyloxy-1,4-androstadiene-3,17-dione with sodium azide in dimethylformamide. Isolate and purify the resultant product in a manner similar to that described to obtain 6-azido-1,4,6-androstatriene-3,17-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931167 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-97e55c828abb40e58cda910f1bad373e |
| Source note | uspto-grants-1976_01 |