HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 54366785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 86732880 | HCID 86732880 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54366785 | HCID 54366785 | — |
Reaction Steps
In a manner similar to that described in Example 6C, treat 6β,7β-dimethanesulfonyloxy-4-cholestene-3-one with sodium azide in aqueous methanol in the presence of acetic acid. Isolate and purify the resultant product in a manner similar to that described to obtain 6-azido-4,6-cholestadiene-3-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931167 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-f64c64f06ca943e3ac79325ca016c376 |
| Source note | uspto-grants-1976_01 |