HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 21490323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | HCID 21568706 | HCID 21568706 | — |
| Product | HCID 21490323 | HCID 21490323 | 24.1% |
Reaction Steps
2-Amino-5-chloro-3-(o-chlorophenyl)-3H-indol-3-ol (5.86 g) was heated under reflux with 1,4-dibromobutane (4.32 g) for 18 hours. On cooling the hydrobromide of the title compound (1.67 g) was deposited m.p. 295°-300°C (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931226 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-59b1481c0ce04a0986037046fa5963d9 |
| Source note | uspto-grants-1976_01 |