HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 53949821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Dichloroacetyl chloride | HCID 6593 | — |
| Reactant | N-Butylidene-2-methyl-2-propanamine | HCID 11332470 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 53949821 | HCID 53949821 | — |
Reaction Steps
In a similar procedure as Example I, 6.6 g. (0.052 mole) N-butylidene-t-butylamine was reacted with 4.8 ml. (0.05 mole) dichloroacetyl chloride in 100 ml. diethyl ether and 7.2 ml. triethylamine. There was obtained 9.3 g. of the title compound, an oil, nD30 = 1.4858.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931313 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-88916a26544e45e29b89dc285d4bcef0 |
| Source note | uspto-grants-1976_01 |