Diethyl Ether → HCID 53949821, compound

HRID 1579735Notes

Reaction equation

HRID 1579735 reaction equation
[CH:1](=[N:5][C:6]([CH3:9])([CH3:8])[CH3:7])[CH2:2][CH2:3][CH3:4].[Cl:10][CH:11]([Cl:15])[C:12](Cl)=[O:13].C(OCC)C>C(N(CC)CC)C>[C:6]([N:5]([CH:1]=[CH:2][CH2:3][CH3:4])[C:12](=[O:13])[CH:11]([Cl:15])[Cl:10])([CH3:9])([CH3:8])[CH3:7]

Participants

5

Reactant 3

HCID 3283Diethyl EtherHCID 6593Dichloroacetyl chlorideHCID 11332470N-Butylidene-2-methyl-2-propanamine

Product 1

HCID 53949821HCID 53949821, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

In a similar procedure as Example I, 6.6 g. (0.052 mole) N-butylidene-t-butylamine was reacted with 4.8 ml. (0.05 mole) dichloroacetyl chloride in 100 ml. diethyl ether and 7.2 ml. triethylamine. There was obtained 9.3 g. of the title compound, an oil, nD30 = 1.4858.

Workup

  1. customThere was obtained 9.3 g

Sources & evidence

ORD record
ord-88916a26544e45e29b89dc285d4bcef0
Source dataset
uspto-grants-1976_01
Patent number
US03931313

Reaction notes

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