HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54159344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Dichloroacetyl chloride | HCID 6593 | — |
| Reactant | N-ethylpentan-3-imine | HCID 351395 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 54159344 | HCID 54159344 | — |
Reaction Steps
In a similar procedure as Example I, 5.9 g. (0.052 mole) N-3-pentylidene ethylamine was reacted with 4.8 ml. (0.05 mole) dichloroacetyl chloride in 100 ml. diethyl ether and 7.2 ml. triethylamine. There was obtained 7.7 g. of the title compound, an oil, nD30 = 1.4826.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931313 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-e049030afc6c4a0ebb6e1eb4c24ce1ad |
| Source note | uspto-grants-1976_01 |