Diethyl Ether → HCID 54159344, compound

HRID 1579736Notes

Reaction equation

HRID 1579736 reaction equation
[CH3:1][CH2:2][C:3](=[N:6][CH2:7][CH3:8])[CH2:4][CH3:5].[Cl:9][CH:10]([Cl:14])[C:11](Cl)=[O:12].C(OCC)C>C(N(CC)CC)C>[CH2:7]([N:6]([C:3](=[CH:4][CH3:5])[CH2:2][CH3:1])[C:11](=[O:12])[CH:10]([Cl:14])[Cl:9])[CH3:8]

Participants

5

Reactant 3

HCID 3283Diethyl EtherHCID 6593Dichloroacetyl chlorideHCID 351395N-ethylpentan-3-imine

Product 1

HCID 54159344HCID 54159344, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

In a similar procedure as Example I, 5.9 g. (0.052 mole) N-3-pentylidene ethylamine was reacted with 4.8 ml. (0.05 mole) dichloroacetyl chloride in 100 ml. diethyl ether and 7.2 ml. triethylamine. There was obtained 7.7 g. of the title compound, an oil, nD30 = 1.4826.

Workup

  1. customThere was obtained 7.7 g

Sources & evidence

ORD record
ord-e049030afc6c4a0ebb6e1eb4c24ce1ad
Source dataset
uspto-grants-1976_01
Patent number
US03931313

Reaction notes

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