HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Methyl-5-(2,6,6-trimethylcyclohex-2-en-1-yl)-1,2-oxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | HCID 86732896 | HCID 86732896 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 3-Methyl-5-(2,6,6-trimethylcyclohex-2-en-1-yl)-1,2-oxazole | HCID 3016056 | — |
Reaction Steps
54 g of 4-[2,6,6-trimethyl-cyclohex-2-en-1-yl]-3,4-epoxy-2-butanone-oxime, which can be prepared as indicated above, in 500 ml of benzene were refluxed in the presence of 2 g of p-toluenesulphonic acid for about 4 hours. The water formed in the course of the reaction was removed as it formed by azeotropic distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931323 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-b2d2b942c7f34a4097ace64b60fbe746 |
| Source note | uspto-grants-1976_01 |