Diethylamine → HCID 131709891, compound

HRID 1579829Notes

Reaction equation

HRID 1579829 reaction equation
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].[CH3:6][O:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][CH:17]=1)[CH:14]=[C:13]([CH:18]([OH:22])[C:19]([OH:21])=[O:20])[CH:12]=[CH:11]2>CCCCCC>[CH2:1]([NH2+:3][CH2:4][CH3:5])[CH3:2].[CH3:6][O:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][CH:17]=1)[CH:14]=[C:13]([CH:18]([OH:22])[C:19]([O-:21])=[O:20])[CH:12]=[CH:11]2

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 21569136HCID 21569136, compound

Product 1

HCID 131709891HCID 131709891, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Procedure

Anhydrous diethylamine (0.11 moles) is added dropwise to a stirred solution of 6-methoxy-2-naphthylglycolic acid (0.10 moles) in 100 ml. of n-hexane at 0°C. The precipitated diethylammonium salt is collected on a filter washed with n-hexane and dried in a vacuum desiccator to obtain 6-methoxy-2-naphthylglycolic acid, diethylammonium salt.

Workup

  1. customat 0°C
  2. customThe precipitated diethylammonium salt is collected on a filter
  3. washwashed with n-hexane
  4. customdried in a vacuum desiccator

Sources & evidence

ORD record
ord-2380ed9d446148df9b302c141e1a8fd4
Source dataset
uspto-grants-1976_01
Patent number
US03931269

Reaction notes

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