HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 21569111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | HCID 21569099 | HCID 21569099 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21569111 | HCID 21569111 | — |
Reaction Steps
A mixture of 0.1 moles of ethyl α-bromo-6-methoxy-2-naphthylacetate and 150 g. of sodium iodide in 1 liter of anhydrous acetone is refluxed for 4 hours. The reaction mixture is then evaporated to dryness and extracted with ether. The ether is then washed with water, dried and evaporated to dryness to obtain ethyl α-iodo-6-methoxy-2-naphthylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931269 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-a4dde2ca43fa468994c7bd2b17823ab8 |
| Source note | uspto-grants-1976_01 |