化工社化工社 化学情報印刷レポート · 研究参考用
5-Aminosalicylic Acid → HCID 9967439、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Aminosalicylic Acid | HCID 4075 | — |
| 反応物 | 2-(2-Oxo-2-phenylethyl)cyclohexanone | HCID 10512899 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | HCID 9967439 | HCID 9967439 | — |
反応手順
A solution of 49.7 g. (0.23 mole) of 2-phenacylcyclohexanone, 35.2 g. (0.23 mole) of 5-aminosalicylic acid, and 135 ml. of glacial acetic acid was heated under reflux under nitrogen for 31/2 hours. A solid separated and was collected, washed with water, and recrystallized from acetic acid to provide 46.0 g. (60%) of pale yellow crystals, m.p. 209°-211°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03931407 |
| 出典データセット | uspto-grants-1976_01 |
| ORD ID | ord-2ec61bad43804fb39d6dbb66d027f5b9 |
| 出典メモ | uspto-grants-1976_01 |