HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Oxo-2-phenylethyl)cyclohexanone → HCID 12270285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Oxo-2-phenylethyl)cyclohexanone | HCID 10512899 | — |
| Reactant | HCID 21569608 | HCID 21569608 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12270285 | HCID 12270285 | — |
Reaction Steps
A mixture of 6.5 g. (0.029 mole) of 5-amino-4-trifluoromethylsalicylic acid, 6.35 g. (0.029 mole) of 2-phenacylcyclohexanone, and 30 ml. of glacial acetic acid was heated under reflux for 3 hours, cooled and filtered. The filter cake was recrystallized from acetic acid to provide 4.6 g. (39%) of gold crystals, m.p. 188°-190°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931407 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-7925a4da242b41b5af123b67a658b254 |
| Source note | uspto-grants-1976_01 |