HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Oxo-2-phenylethyl)cyclohexanone → HCID 12270288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Oxo-2-phenylethyl)cyclohexanone | HCID 10512899 | — |
| Reactant | HCID 12270347 | HCID 12270347 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12270288 | HCID 12270288 | — |
Reaction Steps
A mixture of 10.3 g. (0.048 mole) of 2-phenacylcyclohexanone, 10 g. (0.048 mole) of 3-acetamido-5-aminosalicylic acid, and 70 ml. of glacial acetic acid was heated under reflux under nitrogen for 1 hour, cooled and filtered. Recrystallization of the collected solid from acetic acid gave 10.5 g. (57%) of crystals, m.p. 232°-234°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931407 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-8da86c221c1f4a44830b44b43f570202 |
| Source note | uspto-grants-1976_01 |