反应详情

A mixture of 8.1 g. (0.038 mole) of 2-phenacylcyclohexanone, 8.7 g. (0.038 mole) of 5-amino-3-bromosalicylic acid, and 50 ml. of glacial acetic acid was heated under reflux for 1 hour, cooled and filtered. Recrystallization of the collected solid from acetonitrile gave 7.0 g. (46%) of yellow crystals, m.p. 209°-210°.

1. additionA mixture of 8.1 g
2. temperatureunder reflux for 1 hour
3. temperaturecooled
4. filtrationfiltered
5. customRecrystallization of the collected solid from acetonitrile
6. customgave 7.0 g