HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Oxo-2-phenylethyl)cyclohexanone → HCID 12270286, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Oxo-2-phenylethyl)cyclohexanone | HCID 10512899 | — |
| Reactant | 54669-99-7 | HCID 20327555 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12270286 | HCID 12270286 | — |
Reaction Steps
A mixture of 8.1 g. (0.038 mole) of 2-phenacylcyclohexanone, 8.7 g. (0.038 mole) of 5-amino-3-bromosalicylic acid, and 50 ml. of glacial acetic acid was heated under reflux for 1 hour, cooled and filtered. Recrystallization of the collected solid from acetonitrile gave 7.0 g. (46%) of yellow crystals, m.p. 209°-210°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931407 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-44c2f77f93204f87bb45a32f82c4ed54 |
| Source note | uspto-grants-1976_01 |